压载对M4761单晶高温合金再结晶行为的影响

    Effect of Ballast on Recrystallization Behavior of M4761 Single Crystal Superalloy

    • 摘要: 研究了单晶高温合金M4761浇注完成后的铸态组织特征,以及在不同压载、不同固溶温度下M4761单晶合金再结晶组织演变规律。结果表明:由于凝固偏析的存在,M4761单晶高温合金枝晶干与枝晶间显微组织存在明显的差异,枝晶干γ'尺寸比枝晶间小;M4761单晶高温合金再结晶层深度随着固溶温度、载荷的增加而增大,当固溶温度低于1220℃时,再结晶层深度增加缓慢,接近γ'相溶解温度(约1220℃),再结晶深度增加速度加快;再结晶晶界处,γ'相富集且尺寸较大,从压痕表面到再结晶的晶界处,γ'相的尺寸由小变大,由晶界到合金内部基体处,γ'相均匀分布。固溶温度较高时,γ'相钝化呈球状形貌。

       

      Abstract: The characteristics of the cast microstructure of M4761 single crystal superalloy after pouring and the evolution of the recrystallization microstructure of M4761 single crystal alloy at different ballast and different solution temperatures were investigated.The results show that there are obvious differences in microstructure between M4761 dendrite and M4761 dendrite due to the existence of solidification segregation. The γ' size of the dendrites is smaller than that between the dendrites. The depth of M4761 recrystallization layer increases with increasing temperature and load. When the solution temperature is below 1220 ℃, the depth of recrystallization layer increases slowly. Close to the γ' phase dissolution temperature (about 1220 ℃), the increasing rate of recrystallization depth is accelerated.The γ'phase is enriched and the size is large at recrystallization grain boundaries.From the indentation surface to the recrystallized grain boundary, the size of the γ' phase changes from small to large. From grain boundary to alloy interior matrix, the γ' phase is in uniform distribution.When the solid solution temperature is high, the γ'phase passivation has a spherical morphology.

       

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