用于医用增材制造的Ti6Al4V和Ti6Al4V ELI原材料粉末的质量控制研究

    Study on Quality Control of Ti6Al4V and Ti6Al4V ELI Raw Material Powders Used in Medical Additive Manufacturing

    • 摘要: 对用于医用增材制造的国产Ti6Al4V/Ti6Al4V ELI粉末的特性进行评价和质量控制研究,以期为我国医用增材制造行业提供数据参考。采用经过验证的或者现行标准中的测试方法对Ti6Al4V/Ti6Al4V ELI粉末的化学成分、粒度分布、振实密度、松装密度、流动性等性能进行测试。结果表明:研究所用的国产Ti6Al4V/Ti6Al4V ELI粉末粉末粒径分布较窄,能满足对能量的均匀吸收。化学成分满足GB/T 3620.1—2016和GB/T 13810—2017中的相应要求,用于SLM工艺时的粉末松装密度均不小于2.2 g/cm3、振实密度均不小于2.5g/cm3、流动性均不大于50 s/50 g。用于EBM工艺时的粉末松装密度均不小于2.3 g/cm3、振实密度均不小于2.5 g/cm3、流动性均不大于30 s/50 g。

       

      Abstract: The properties and quality control of Ti6Al4V/Ti6Al4V ELI powder used in medical additive manufacturing were evaluated, in order to provide data reference for the medical additive manufacturing industry in China. The chemical composition, particle size distribution, vibrational density, loose density, fluidity and other properties of Ti6Al4V/Ti6Al4V ELI powders were tested and compared by the tested or current standard test methods. The results show that the particle size distribution of domestic Ti6Al4V/Ti6Al4V ELI powders used in this study is narrow and can meet the requirement of uniform energy absorption. The chemical composition meets the corresponding requirements in GB/T 3620.1—2016 and GB/T13810—2017. The powder bulk density used in SLM process is not less than 2.2 g/cm~3, the vibrational density is not less than2.5 g/cm3, and the fluidity is not more than 50 s/50 g. The bulk density of powder used in EBM process is not less than 2.3g/cm~3, the vibrational density is not less than 2.5 g/cm~3, and the fluidity is not more than 30 s/50 g.

       

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