Fe-3.2% Si-0.055% Nb取向硅钢热轧与常化过程中组织与织构演变

    Microstructure and Texture Evolution of Fe-3.2%Si-0.055% Nb Grain-oriented Silicon Steel during Hot Rolling and Normalizing

    • 摘要: 采用OM和EBSD研究了常化处理对含0.055%Nb的Fe-3.2%Si-0.055%Nb低温取向硅钢抑制剂、组织、织构和晶界特征的影响。结果表明:热轧板组织沿厚度方向呈条带状分布并且梯度性明显,在常化后组织的不均匀性变缓和,显微组织以铁素体为主,并在晶界处存在含量较少的渗碳体;常化工艺极大地改善了取向硅钢热轧板中抑制剂的数量及分布情况,使得抑制剂更加弥散且细小的析出;热轧板和常化板织构的类型和织构的取向密度有很大的区别,与热轧板相比常化板γ线织构的强度较弱,而且旋转立方织构的强度也较弱,常化板织构的分布比较散漫;热轧板晶界类型以小角度晶界为主,高能晶界和大角度晶界的含量较少,而热轧板常化后,试样晶界类型则主要以高能晶界为主,并且晶界能和迁移率较高的Σ9和Σ13b晶界在常化后含量大幅增加。热轧板经常化处理后更有利于后续高温退火中Goss晶粒的异常长大。

       

      Abstract: The effects of normalizing treatment on the inhibitor, microstructure, texture and grain boundary characteristics of Fe-3.2%Si-0.055%Nb low temperature grain-oriented silicon steel containing 0.055% Nb were studied by OM and EBSD techniques. The results show that the structure of the hot rolled plate is distributed in strips along the thickness direction and the gradient is obvious. After normalization, the heterogeneity of the structure becomes mild. The microstructure is mainly ferrite and there is less cementite at the grain boundary. The normalization process greatly improves the quantity and distribution of inhibitors in the hot rolled plate of grain-oriented silicon steel, making the inhibitors more dispersed and fine precipitation. There are great differences in texture types and orientation density between hot-rolled plate and normalized plateγ. The strength of linear texture is weak, and the strength of rotating cube texture is also weak, and the distribution of normalized plate texture is scattered. The grain boundary type of hot-rolled plate is mainly small angle grain boundary, and the content of high-energy grain boundary and large angle grain boundary is less. After the normalization of hot-rolled plate, the grain boundary type of sample is mainly high-energy grain boundary, Σ9 and Σ13b grain boundaries with higher grain boundary energy and mobility increase significantly after normalization. Normalizing treatment is more conducive to the abnormal growth of Goss grains in subsequent high-temperature annealing.

       

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