预回复退火工艺对薄规格无取向硅钢组织与织构的影响

    Effect of Pre-recovery Annealing on Microstructure and Texture of Thin-gauge Non-oriented Silicon Steel

    • 摘要: 对铸轧薄规格无取向硅钢分别进行直接再结晶退火和包含预回复退火的两阶段退火工艺,利用光学显微镜、EBSD和X射线衍射研究了退火工艺对无取向硅钢再结晶组织和织构的影响。结果表明:直接再结晶退火时,再结晶织构为强的γ和α'织构,再结晶组织的平均晶粒尺寸仅为65.1μm。引入预回复退火后,随着预回复退火温度升高,再结晶组织的平均晶粒尺寸逐渐增大至87.3μm。此外,γ再结晶织构逐渐减弱,λ再结晶织构逐渐增强。经550℃预退火的再结晶组织中100织构体积分数达42.3%,比直接再结晶退火提高31.7%。

       

      Abstract: Casting-rolling thin-gauge non-oriented silicon steel was subjected to direct recrystallization annealing and a two-stage annealing process including pre-recovery annealing process, respectively. The effects of annealing process on recrystallized microstructure and texture of non-oriented silicon steel were studied by optical microscope, EBSD and X-ray diffraction. The results show that the microstructure after direct recrystallization annealing exhibits strong γ-fiber and α’-fiber texture, and the average grain size is only 65.1 μm. After introducing pre-recovery annealing, the average grain size of the recrystallized structure gradually increases to 87.3 μm with the increase of pre-annealing temperature. In addition, the γ-fiber recrystallization texture is gradually weakened, while the λ-fiber texture is gradually enhanced. The volume fraction of 100texture in the recrystallized microstructure subjected pre-annealing at 550 ℃ reaches 42.3%, which is 31.7% higher than that of direct recrystallization annealing.

       

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