M2/Ti粉末高速钢的烧结组织转变与性能研究

    Study on Microstructure Transformation and Properties of High Speed Steel Sintered by M2/Ti Powders

    • 摘要: 采用机械合金化制备了M2与Ti的混合粉末,粉末经模压成型后真空烧结,得到含Ti的烧结合金。研究烧结试样的致密化行为、显微组织和力学性能。结果表明,湿磨之后的M2和Ti混合粉末呈鹅卵石状,中值粒径为15.5μm,Ti元素均匀分布于粉末基体中。在900~1030℃烧结时,烧结试样致密度低,大量细小的M6C碳化物均匀分布在基体中,碳化物尺寸较小。随着烧结温度的提高,试样的致密度增加,孔隙减少,试样中原有的碳化物长大,更多的细小碳化物析出。在1110~1150℃烧结时,组织均匀化程度降低,M6C碳化物长大,呈不规则状且数量减少,MC碳化物含量增加。烧结温度的提高,使碳化物长大明显,有团聚现象,黑色碳化物颗粒和MC碳化物在M6C碳化物周围密集产生。试样的表观硬度随着烧结温度升高而提高,1150℃的烧结材料具有最高的硬度(55.2 HRC),抗弯强度先升后降,1140℃烧结时最高,为1556 MPa。

       

      Abstract: The mixed powders of Ti and M2 were prepared by using mechanical alloying method, which was molded and then sintered under vacuum circumstance, then the sintered alloy containing Ti was obtained. The densification behavior,microstructure and mechanical properties of the sintered samples were studied. The results show that the mixed powder of M2 and Ti after wet grinding is pebble-like with a medium particle size of 15.5 μm, and Ti element is evenly distributed in the powder matrix. When it is sintered at 900-1030 ℃, the sintered samples have low density, and a large number of fine M6C carbides are uniformly distributed in the matrix, and the carbide size is small. With the increase of the sintering temperature,the density of the sample increases, the porosity decreases, the original carbides in the sample grow, and more fine carbides precipitate. When it is sintered at 1110-1150 ℃, the structure homogenization decreases, the M6C carbides grow to irregular and the content of MC carbides increases. The increase of sintering temperature make the carbides grow obviously, and the carbides are agglomerated, black carbide particles and MC carbides are densely formed around the M6C carbides. Apparent hardness of the sample increases with the increase of sintering temperature. The material sintered at 1150 ℃ has the highest hardness of 55.2 HRC. The bending strength rises first and then falls, and the material sintered at 1140 ℃ has the maximum bending strength of 1556 MPa.

       

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