原位自生(TiC+TiB)增强钛基复合材料的热变形行为研究

    Study on Hot Deformation Behavior of In-situ TiC+TiB Reinforced Titanium Matrix Composites

    • 摘要: 在Gleeble-3800热模拟试验机上进行了原位自生10vol%(TiC+TiB)增强钛基复合材料的热压缩变形试验,研究了变形温度为750~900℃、应变速率为0.001~1 s-1的钛基复合材料的热变形行为,并使用扫描电子显微镜(SEM)和透射电子显微镜(TEM)观察了该复合材料变形后的显微组织演变。结果表明:该复合材料的流变曲线均依次出现加工硬化、流变软化、稳态流变3个阶段,流变应力和峰值应力均随着变形温度的升高和应变速率的降低而降低。构建了基于不同变形条件下峰值应力的复合材料本构方程,相关系数达到0.96以上。随着变形温度的升高,α相含量逐渐减少,β相含量增多;在动态回复和动态再结晶阶段会形成位错墙,并且温度的升高有利于提高钛基体和增强相的协同变形,进而提高材料的性能。

       

      Abstract: The thermal deformation behavior of in-situ 10vol%(TiC +TiB) reinforced titanium matrix composites was investigated at the temperature of 750-900 ℃ and strain rate of 0.001-1 s-1on the Gleeble-3800 thermal simulation testing machine by the hot compression deformation test. The microstructure evolution of the composites after deformation was observed using SEM and TEM. The results show that the flow curves of the composites exhibit three stages: work hardening,flow softening and steady-state flow, and the flow stress and peak stress decrease with the increase of deformation temperature and decrease of strain rate. And a constitutive equation of composites based on peak stress under different deformation conditions was constructed, with a correlation coefficient of over 0.96. As the deformation temperature increases,the α phase content gradually decreases, while the β phase content increases. During the dynamic recovery and dynamic recrystallization stages, the dislocation walls are formed, and the temperature increase is beneficial for improving the coordinated deformation of titanium matrix and reinforcing phases, and thereby improving the material properties.

       

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