固溶与轧制工艺对GH4738高温合金晶粒异常长大的影响

    Effect of Solution and Rolling Process on Abnormal Grain Growth of GH4738 Superalloy

    • 摘要: 基于固溶热处理和楔形试样轧制实验,研究了固溶温度、轧制温度和变形量对GH4738高温合金晶粒异常长大的影响。结果表明:随着固溶温度的升高,合金的平均晶粒尺寸逐渐增大。采用亚固溶热处理(1030℃)后的楔形试样经不同轧制温度和变形量热轧后,其组织相对细小均匀,未出现异常晶粒长大现象。而采用过固溶热处理(1080℃和1120℃)后的楔形试样经不同轧制温度和变形量热轧后,在变形量为10%和20%处发生了晶粒异常长大。合金发生晶粒异常长大的临界变形温度为1060℃,临界变形量为10%~20%,选择20%及以上的变形量,可以有效避免晶粒异常长大,获得均匀的晶粒组织。当固溶温度一定时,随着轧制变形量的增加,合金的硬度逐渐增加。当轧制温度一定时,随着固溶温度的升高,合金硬度逐渐降低。研究结果对GH4738高温合金晶粒异常长大的控制具有重要意义。

       

      Abstract: The effects of solution temperatures, rolling temperatures and deformation amounts on the abnormal grain growth(AGG) in GH4738 superalloy were investigated through solution heat treatment and wedge-shaped sample rolling experiments. The results indicate that the average grain size of the alloy gradually increases with the rise of solution temperature. Wedge-shaped samples subjected to sub-solid solution heat treatment at 1030 ℃ and hot rolling at various rolling temperatures and deformation amounts, exhibit relatively fine and uniform microstructures, with no abnormal grain growth observed. However, wedge-shaped samples treated with sup-solid solution heat treatments at 1080 ℃ and 1120 ℃ and hot rolling under varying conditions, show abnormal grain growth at deformation amounts of 10% and 20%. The critical temperature for abnormal grain growth in the alloy is determined to be 1060 ℃, with a critical deformation amount between 10% and 20%. Selecting a deformation amount of 20% or higher can effectively prevent abnormal grain growth, resulting in a uniform grain structure. When the solution temperature is constant, the hardness of the alloy gradually increases with the increase of rolling deformation. However, when the rolling temperature is constant, the hardness of the alloy gradually decreases with the increase of solution temperature. The research results provide important guidance for controlling abnormal grain growth in GH4738 superalloy.

       

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