L-PBF超细粒径粉末增材制造共晶高熵合金的微观组织表征与力学性能

    Microstructure Characterization and Mechanical Properties of Eutectic High-entropy Alloys Fabricated by L-PBF Ultrafine Particle Size Powder Additive Manufacturing

    • 摘要: 采用激光粉末床熔融技术(L-PBF)制备了AlCoCrFeNi2.1共晶高熵合金(EHEAs),研究了L-PBF参数对合金成形性的影响、成形试样独特的双相微观结构和力学性能。结果表明:结合L-PBF工艺参数,当体积能量密度VED=119 J/mm3时,AlCoCrFeNi2.1 EHEAs的致密度最高,可达到99.38%,不同表面粗糙度最低。通过L-PBF打印的AlCoCrFeNi2.1 EHEAs由FCC和BCC/B2相组成,颗粒状B2相弥散分布于BCC基体中。由于凝固过程中冷却速率变化和层间热传导的共同作用,在凝固熔池不同位置共存有共晶层状结构、柱状晶和胞状晶。L-PBF打印AlCoCrFeNi2.1 EHEAs显微硬度与成形精度密切相关,最大硬度为VED=119 J/mm3试样的425 HV,试样抗拉强度为1127 MPa,塑性为14.1%。由于FCC与BCC/B2两相之间的变形不协调,平直相界限制了位错滑移,实现了强度与塑性的良好匹配。

       

      Abstract: AlCoCrFeNi2.1 eutectic high entropy alloys (EHEAs) were prepared by laser powder bed fusion (L-PBF) technology, the effects of L-PBF parameters on the formability of the alloys, the unique duplex microstructures and the mechanical properties of the formed specimens were investigated. The results show that, combining the L-PBF process parameters, AlCoCrFeNi2.1 EHEAs indicate the highest densification up to 99.38% and the lowest different surface roughness when volumetric energy density(VED) VED=119 J/mm3. The AlCoCrFeNi2.1 EHEAs printed by L-PBF consist of FCC and BCC/B2 phases, the particulate B2 phase diffusely distributes in the BCC matrix. As a result of changes in cooling rate and interlayer heat transfer during solidification, eutectic lamellar structures, columnar crystals and cellular crystals coexist at different locations in the solidification melt pool. The microhardness of AlCoCrFeNi2.1 EHEAs Printed by L-PBF is closely related to the forming accuracy, and the maximum hardness of VED 119 sample is 425 HV, the tensile strength is 1127 MPa and the plasticity is 14.1%. Due to the deformation incoherence between FCC and BCC/B2 phases, the flat phase boundary limits the dislocation slip and achieves a good match between strength and plasticity.

       

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